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Study of deformation mechanisms in flash-sintered yttria-stabilized zirconia by in-situ micromechanical testing at elevated temperatures

  • Jaehun Cho
  • , Jin Li
  • , Han Wang
  • , Qiang Li
  • , Zhe Fan
  • , A. K. Mukherjee
  • , W. Rheinheimer
  • , Haiyan Wang*
  • , X. Zhang
  • *Corresponding author for this work
  • Purdue University
  • Oak Ridge National Laboratory
  • University of California at Davis

Research output: Contribution to journalArticlepeer-review

Abstract

Flash sintering has received wide attention lately due to its ultrafast densification process at low sintering temperature. However, the deformability of flash-sintered ceramics remains poorly understood. Yttria-stabilized zirconia (YSZ) was processed by flash sintering to study deformation mechanism. Transmission electron microscopy studies show that the flash-sintered YSZ contains ultrafine grains and dislocations. Strain rate jump tests at elevated temperature by in-situ microcompression indicate the existence of a large threshold stress. The activation energy of deformation is ∼145 kJ/mol, similar to the activation energy for oxygen vacancy migration. The deformation mechanisms of the flash-sintered YSZ at elevated temperatures are discussed. IMPACT STATEMENT: The current study reveals the underlying deformation mechanisms of flash-sintered 3YSZ that shows considerable plasticity over the temperature range of 450–650°C via in-situ microcompression test.

Original languageEnglish
Pages (from-to)194-202
Number of pages9
JournalMaterials Research Letters
Volume7
Issue number5
DOIs
StatePublished - 4 May 2019
Externally publishedYes

Keywords

  • Flash sintering
  • deformation mechanism
  • dislocation
  • in-situ microcompression test

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