Solvothermal growth of NiS single-crystalline nanorods

Pengfei Yang; B. Song; R. Wu; Yufeng Zheng; Yanfei Sun; J. K. Jian

doi:10.1016/j.jallcom.2009.02.154

Solvothermal growth of NiS single-crystalline nanorods

Pengfei Yang
, B. Song
, R. Wu
, Yufeng Zheng
, Yanfei Sun
, J. K. Jian^*

^*Corresponding author for this work

School of Astronautics

Xinjiang University
CAS - Institute of Physics

Research output: Contribution to journal › Article › peer-review

23 Scopus citations

Abstract

Nanorods of NiS were successfully prepared by a solvothermal synthetic route using S and Ni powders as reagents in ethylenediamine (en) solvent at the temperature of 200 °C. The as prepared NiS nanorods were characterized by X-ray diffraction (XRD), field emission scanning electron microscopy (FE-SEM) and transmission electron microscopy (TEM). It was found that the nanorods have diameters and lengths in the region from 80 nm to 120 nm, and from 2 μm to 3 μm, respectively. The NiS nanorods are single crystals with millerite structure. On the basis of the experimental results and corresponding literatures, a possible growth mechanism of the NiS nanorods crystals is discussed.

Original language	English
Pages (from-to)	450-454
Number of pages	5
Journal	Journal of Alloys and Compounds
Volume	481
Issue number	1-2
DOIs	https://doi.org/10.1016/j.jallcom.2009.02.154
State	Published - 29 Jul 2009

Keywords

Crystal growth
Nanostructures
Scanning and transmission electron microscopy

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10.1016/j.jallcom.2009.02.154

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title = "Solvothermal growth of NiS single-crystalline nanorods",

abstract = "Nanorods of NiS were successfully prepared by a solvothermal synthetic route using S and Ni powders as reagents in ethylenediamine (en) solvent at the temperature of 200 °C. The as prepared NiS nanorods were characterized by X-ray diffraction (XRD), field emission scanning electron microscopy (FE-SEM) and transmission electron microscopy (TEM). It was found that the nanorods have diameters and lengths in the region from 80 nm to 120 nm, and from 2 μm to 3 μm, respectively. The NiS nanorods are single crystals with millerite structure. On the basis of the experimental results and corresponding literatures, a possible growth mechanism of the NiS nanorods crystals is discussed.",

keywords = "Crystal growth, Nanostructures, Scanning and transmission electron microscopy",

author = "Pengfei Yang and B. Song and R. Wu and Yufeng Zheng and Yanfei Sun and Jian, \{J. K.\}",

year = "2009",

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doi = "10.1016/j.jallcom.2009.02.154",

language = "英语",

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pages = "450--454",

journal = "Journal of Alloys and Compounds",

issn = "0925-8388",

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}

TY - JOUR

T1 - Solvothermal growth of NiS single-crystalline nanorods

AU - Yang, Pengfei

AU - Song, B.

AU - Wu, R.

AU - Zheng, Yufeng

AU - Sun, Yanfei

AU - Jian, J. K.

PY - 2009/7/29

Y1 - 2009/7/29

N2 - Nanorods of NiS were successfully prepared by a solvothermal synthetic route using S and Ni powders as reagents in ethylenediamine (en) solvent at the temperature of 200 °C. The as prepared NiS nanorods were characterized by X-ray diffraction (XRD), field emission scanning electron microscopy (FE-SEM) and transmission electron microscopy (TEM). It was found that the nanorods have diameters and lengths in the region from 80 nm to 120 nm, and from 2 μm to 3 μm, respectively. The NiS nanorods are single crystals with millerite structure. On the basis of the experimental results and corresponding literatures, a possible growth mechanism of the NiS nanorods crystals is discussed.

AB - Nanorods of NiS were successfully prepared by a solvothermal synthetic route using S and Ni powders as reagents in ethylenediamine (en) solvent at the temperature of 200 °C. The as prepared NiS nanorods were characterized by X-ray diffraction (XRD), field emission scanning electron microscopy (FE-SEM) and transmission electron microscopy (TEM). It was found that the nanorods have diameters and lengths in the region from 80 nm to 120 nm, and from 2 μm to 3 μm, respectively. The NiS nanorods are single crystals with millerite structure. On the basis of the experimental results and corresponding literatures, a possible growth mechanism of the NiS nanorods crystals is discussed.

KW - Crystal growth

KW - Nanostructures

KW - Scanning and transmission electron microscopy

UR - https://www.scopus.com/pages/publications/67649267349

U2 - 10.1016/j.jallcom.2009.02.154

DO - 10.1016/j.jallcom.2009.02.154

M3 - 文章

AN - SCOPUS:67649267349

SN - 0925-8388

VL - 481

SP - 450

EP - 454

JO - Journal of Alloys and Compounds

JF - Journal of Alloys and Compounds

IS - 1-2

ER -

Solvothermal growth of NiS single-crystalline nanorods

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Keywords

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