Quantitative determination of free TDI content in crosslinker by GC-MS

Ju Sheng Zhang; Shuang Hua Guo; Zhi Gang Liu; Ji Feng Zhang; Xue Tian Gao; Qing Na Huang

Quantitative determination of free TDI content in crosslinker by GC-MS

Ju Sheng Zhang^*
, Shuang Hua Guo
, Zhi Gang Liu
, Ji Feng Zhang
, Xue Tian Gao
, Qing Na Huang

^*Corresponding author for this work

School of Chemistry and Chemical Engineering

Harbin Institute of Technology

Research output: Contribution to journal › Article › peer-review

1 Scopus citations

Abstract

The free toluene diisocyanate (TDI) in TDI-TMP crosslinker must be controlled due to its considerable harm on human. Firstly, the content of free TDI in crosslinker was produced by distillation in vacuum. Secondly, the Structure and content of free toluene diisocyanate (TDI) in TDI-TMP crosslinker were characterized by GC-MS. The results show that the aim product is 2, 6-TDI. Its content is below the national standard of 0.5% in China, coincident with the result detected by IR spectrum. The structure and content of free TDI in crosslinker can be characterized by GC-MS easily and accurately.

Original language	English
Pages (from-to)	55-57
Number of pages	3
Journal	Cailiao Kexue yu Gongyi/Material Science and Technology
Volume	17
Issue number	1
State	Published - Feb 2009

Keywords

GC-MS
TDI-TMP crosslinker
Toluene diisocyanate

Cite this

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title = "Quantitative determination of free TDI content in crosslinker by GC-MS",

abstract = "The free toluene diisocyanate (TDI) in TDI-TMP crosslinker must be controlled due to its considerable harm on human. Firstly, the content of free TDI in crosslinker was produced by distillation in vacuum. Secondly, the Structure and content of free toluene diisocyanate (TDI) in TDI-TMP crosslinker were characterized by GC-MS. The results show that the aim product is 2, 6-TDI. Its content is below the national standard of 0.5\% in China, coincident with the result detected by IR spectrum. The structure and content of free TDI in crosslinker can be characterized by GC-MS easily and accurately.",

keywords = "GC-MS, TDI-TMP crosslinker, Toluene diisocyanate",

author = "Zhang, \{Ju Sheng\} and Guo, \{Shuang Hua\} and Liu, \{Zhi Gang\} and Zhang, \{Ji Feng\} and Gao, \{Xue Tian\} and Huang, \{Qing Na\}",

year = "2009",

month = feb,

language = "英语",

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TY - JOUR

T1 - Quantitative determination of free TDI content in crosslinker by GC-MS

AU - Zhang, Ju Sheng

AU - Guo, Shuang Hua

AU - Liu, Zhi Gang

AU - Zhang, Ji Feng

AU - Gao, Xue Tian

AU - Huang, Qing Na

PY - 2009/2

Y1 - 2009/2

N2 - The free toluene diisocyanate (TDI) in TDI-TMP crosslinker must be controlled due to its considerable harm on human. Firstly, the content of free TDI in crosslinker was produced by distillation in vacuum. Secondly, the Structure and content of free toluene diisocyanate (TDI) in TDI-TMP crosslinker were characterized by GC-MS. The results show that the aim product is 2, 6-TDI. Its content is below the national standard of 0.5% in China, coincident with the result detected by IR spectrum. The structure and content of free TDI in crosslinker can be characterized by GC-MS easily and accurately.

AB - The free toluene diisocyanate (TDI) in TDI-TMP crosslinker must be controlled due to its considerable harm on human. Firstly, the content of free TDI in crosslinker was produced by distillation in vacuum. Secondly, the Structure and content of free toluene diisocyanate (TDI) in TDI-TMP crosslinker were characterized by GC-MS. The results show that the aim product is 2, 6-TDI. Its content is below the national standard of 0.5% in China, coincident with the result detected by IR spectrum. The structure and content of free TDI in crosslinker can be characterized by GC-MS easily and accurately.

KW - GC-MS

KW - TDI-TMP crosslinker

KW - Toluene diisocyanate

UR - https://www.scopus.com/pages/publications/64749091927

M3 - 文章

AN - SCOPUS:64749091927

SN - 1005-0299

VL - 17

SP - 55

EP - 57

JO - Cailiao Kexue yu Gongyi/Material Science and Technology

JF - Cailiao Kexue yu Gongyi/Material Science and Technology

IS - 1

ER -

Quantitative determination of free TDI content in crosslinker by GC-MS

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