Interfacial microstructure of Si3N4/Si 3N4 joint brazed using Au-Ni-V filler alloy

J. Zhang; Y. Sun; C. F. Liu; H. W. Zhang

doi:10.1007/s10853-009-4132-1

Interfacial microstructure of Si₃N₄/Si ₃N₄ joint brazed using Au-Ni-V filler alloy

J. Zhang^*
, Y. Sun
, C. F. Liu
, H. W. Zhang

^*Corresponding author for this work

Harbin Institute of Technology

Research output: Contribution to journal › Article › peer-review

11 Scopus citations

Abstract

By using Au58.74Ni36.50V4.76 at.% filler alloy, a reliable Si ₃N₄/Si₃N₄ joint was brazed at 1,423 K for 60 min in vacuum. The microstructure of the joint was investigated and analyzed by scanning electron microscope with energy dispersive spectroscopy, transmission electron microscopy, and X-ray diffraction. The results indicate that the joint consists of three main phases: a continuous VN reaction layer between filler alloy and Si₃N₄ ceramic; an Au[Ni] solid solution as the matrix of the joint; and Ni[Si,V] solid solution particles distributed homogeneously in the Au[Ni] solid solution. The mechanism of formation of the interfacial structure is discussed.

Original language	English
Pages (from-to)	2188-2193
Number of pages	6
Journal	Journal of Materials Science
Volume	45
Issue number	8
DOIs	https://doi.org/10.1007/s10853-009-4132-1
State	Published - Apr 2010
Externally published	Yes

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@article{6c5b66362319450f9cbed9f9581e553d,

title = "Interfacial microstructure of Si3N4/Si 3N4 joint brazed using Au-Ni-V filler alloy",

abstract = "By using Au58.74Ni36.50V4.76 at.\% filler alloy, a reliable Si 3N4/Si3N4 joint was brazed at 1,423 K for 60 min in vacuum. The microstructure of the joint was investigated and analyzed by scanning electron microscope with energy dispersive spectroscopy, transmission electron microscopy, and X-ray diffraction. The results indicate that the joint consists of three main phases: a continuous VN reaction layer between filler alloy and Si3N4 ceramic; an Au[Ni] solid solution as the matrix of the joint; and Ni[Si,V] solid solution particles distributed homogeneously in the Au[Ni] solid solution. The mechanism of formation of the interfacial structure is discussed.",

author = "J. Zhang and Y. Sun and Liu, \{C. F.\} and Zhang, \{H. W.\}",

year = "2010",

month = apr,

doi = "10.1007/s10853-009-4132-1",

language = "英语",

volume = "45",

pages = "2188--2193",

journal = "Journal of Materials Science",

issn = "0022-2461",

publisher = "Springer",

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TY - JOUR

T1 - Interfacial microstructure of Si3N4/Si 3N4 joint brazed using Au-Ni-V filler alloy

AU - Zhang, J.

AU - Sun, Y.

AU - Liu, C. F.

AU - Zhang, H. W.

PY - 2010/4

Y1 - 2010/4

N2 - By using Au58.74Ni36.50V4.76 at.% filler alloy, a reliable Si 3N4/Si3N4 joint was brazed at 1,423 K for 60 min in vacuum. The microstructure of the joint was investigated and analyzed by scanning electron microscope with energy dispersive spectroscopy, transmission electron microscopy, and X-ray diffraction. The results indicate that the joint consists of three main phases: a continuous VN reaction layer between filler alloy and Si3N4 ceramic; an Au[Ni] solid solution as the matrix of the joint; and Ni[Si,V] solid solution particles distributed homogeneously in the Au[Ni] solid solution. The mechanism of formation of the interfacial structure is discussed.

AB - By using Au58.74Ni36.50V4.76 at.% filler alloy, a reliable Si 3N4/Si3N4 joint was brazed at 1,423 K for 60 min in vacuum. The microstructure of the joint was investigated and analyzed by scanning electron microscope with energy dispersive spectroscopy, transmission electron microscopy, and X-ray diffraction. The results indicate that the joint consists of three main phases: a continuous VN reaction layer between filler alloy and Si3N4 ceramic; an Au[Ni] solid solution as the matrix of the joint; and Ni[Si,V] solid solution particles distributed homogeneously in the Au[Ni] solid solution. The mechanism of formation of the interfacial structure is discussed.

UR - https://www.scopus.com/pages/publications/77949873467

U2 - 10.1007/s10853-009-4132-1

DO - 10.1007/s10853-009-4132-1

M3 - 文章

AN - SCOPUS:77949873467

SN - 0022-2461

VL - 45

SP - 2188

EP - 2193

JO - Journal of Materials Science

JF - Journal of Materials Science

IS - 8

ER -

Interfacial microstructure of Si₃N₄/Si ₃N₄ joint brazed using Au-Ni-V filler alloy

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