Hydroxyapatite formation on oxide films containing Ca and P by hydrothermal treatment

Fu Liu; Fuping Wang; Tadao Shimizu; Kaoru Igarashi; Liancheng Zhao

doi:10.1016/j.ceramint.2005.04.006

Hydroxyapatite formation on oxide films containing Ca and P by hydrothermal treatment

Fu Liu^*
, Fuping Wang
, Tadao Shimizu
, Kaoru Igarashi
, Liancheng Zhao

^*Corresponding author for this work

Research output: Contribution to journal › Article › peer-review

58 Scopus citations

Abstract

Oxide films were formed on titanium by means of microarc oxidation (MAO) using a direct current power supply. The oxide films containing Ca and P were obtained in an electrolyte containing β-glycerophosphate sodium salt pentahydrate (β-GP) and calcium acetate (CA). The surfaces of the oxide films were rough and porous, and the concentration of Ca and P were 7.3 mol% and 6.4 mol%, respectively, when MAO was performed in an electrolyte containing 0.04 M β-GP and 0.10 M CA at 200 A/m² current density and 430 V final voltage. The oxide film consists of anatase, rutile and an amorphous phase. After hydrothermal treatment at 190 °C, the hydroxyapatite crystals were precipitated on the oxide film surfaces. The amount of hydroxyapatite crystals increased by increasing the hydrothermal treatment time and the Ca/P ratio in the oxide film.

Original language	English
Pages (from-to)	527-531
Number of pages	5
Journal	Ceramics International
Volume	32
Issue number	5
DOIs	https://doi.org/10.1016/j.ceramint.2005.04.006
State	Published - 2006
Externally published	Yes

Keywords

D. TiO
Hydroxyapatite
Microarc oxidation

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10.1016/j.ceramint.2005.04.006

Cite this

@article{b6b895222c3f4d4a91fa5e6f15027ec5,

title = "Hydroxyapatite formation on oxide films containing Ca and P by hydrothermal treatment",

abstract = "Oxide films were formed on titanium by means of microarc oxidation (MAO) using a direct current power supply. The oxide films containing Ca and P were obtained in an electrolyte containing β-glycerophosphate sodium salt pentahydrate (β-GP) and calcium acetate (CA). The surfaces of the oxide films were rough and porous, and the concentration of Ca and P were 7.3 mol\% and 6.4 mol\%, respectively, when MAO was performed in an electrolyte containing 0.04 M β-GP and 0.10 M CA at 200 A/m2 current density and 430 V final voltage. The oxide film consists of anatase, rutile and an amorphous phase. After hydrothermal treatment at 190 °C, the hydroxyapatite crystals were precipitated on the oxide film surfaces. The amount of hydroxyapatite crystals increased by increasing the hydrothermal treatment time and the Ca/P ratio in the oxide film.",

keywords = "D. TiO, Hydroxyapatite, Microarc oxidation",

author = "Fu Liu and Fuping Wang and Tadao Shimizu and Kaoru Igarashi and Liancheng Zhao",

year = "2006",

doi = "10.1016/j.ceramint.2005.04.006",

language = "英语",

volume = "32",

pages = "527--531",

journal = "Ceramics International",

issn = "0272-8842",

publisher = "Elsevier Ltd",

number = "5",

}

TY - JOUR

T1 - Hydroxyapatite formation on oxide films containing Ca and P by hydrothermal treatment

AU - Liu, Fu

AU - Wang, Fuping

AU - Shimizu, Tadao

AU - Igarashi, Kaoru

AU - Zhao, Liancheng

PY - 2006

Y1 - 2006

N2 - Oxide films were formed on titanium by means of microarc oxidation (MAO) using a direct current power supply. The oxide films containing Ca and P were obtained in an electrolyte containing β-glycerophosphate sodium salt pentahydrate (β-GP) and calcium acetate (CA). The surfaces of the oxide films were rough and porous, and the concentration of Ca and P were 7.3 mol% and 6.4 mol%, respectively, when MAO was performed in an electrolyte containing 0.04 M β-GP and 0.10 M CA at 200 A/m2 current density and 430 V final voltage. The oxide film consists of anatase, rutile and an amorphous phase. After hydrothermal treatment at 190 °C, the hydroxyapatite crystals were precipitated on the oxide film surfaces. The amount of hydroxyapatite crystals increased by increasing the hydrothermal treatment time and the Ca/P ratio in the oxide film.

AB - Oxide films were formed on titanium by means of microarc oxidation (MAO) using a direct current power supply. The oxide films containing Ca and P were obtained in an electrolyte containing β-glycerophosphate sodium salt pentahydrate (β-GP) and calcium acetate (CA). The surfaces of the oxide films were rough and porous, and the concentration of Ca and P were 7.3 mol% and 6.4 mol%, respectively, when MAO was performed in an electrolyte containing 0.04 M β-GP and 0.10 M CA at 200 A/m2 current density and 430 V final voltage. The oxide film consists of anatase, rutile and an amorphous phase. After hydrothermal treatment at 190 °C, the hydroxyapatite crystals were precipitated on the oxide film surfaces. The amount of hydroxyapatite crystals increased by increasing the hydrothermal treatment time and the Ca/P ratio in the oxide film.

KW - D. TiO

KW - Hydroxyapatite

KW - Microarc oxidation

UR - https://www.scopus.com/pages/publications/33646061966

U2 - 10.1016/j.ceramint.2005.04.006

DO - 10.1016/j.ceramint.2005.04.006

M3 - 文章

AN - SCOPUS:33646061966

SN - 0272-8842

VL - 32

SP - 527

EP - 531

JO - Ceramics International

JF - Ceramics International

IS - 5

ER -

Hydroxyapatite formation on oxide films containing Ca and P by hydrothermal treatment

Abstract

Keywords

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