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High-temperature electrochemical synthesis of zirconium diboride powders from chloride-fluoride melts

  • S. A. Kuznetsov
  • , A. L. Glagolevskaya
  • , A. T. Belyaevskii
  • , S. V. Devyatkin
  • , D. Kaptai

Research output: Contribution to journalArticlepeer-review

Abstract

Zirconium diboride powders were obtained by electrolysis of a molten KCl-KF eutectic mixture, containing 15 wt % K2ZrF6 and 15 wt % KBF4, in the range of cathode current density from 0.3 to 1.0 A cm-2 at 1023 K. The effect of cathode current density on the average size of zirconium diboride crystals was studied.

Original languageEnglish
Pages (from-to)1564-1567
Number of pages4
JournalRussian Journal of Applied Chemistry
Volume70
Issue number10
StatePublished - 1997

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