Abstract
Cu0.2Ni0.8O nano-particles and their nano-hybrids were synthesized by wet chemical methods and examined by X-ray diffraction (XRD) technique, spectroscopic analysis, Field Emission scanning electron microscopic (FESEM) technique and energy dispersive x-rays (EDX) analysis. XRD results confirmed that the synthesized materials were crystallite in the cubic phase of Cu0.2Ni0.8O nano-particles annealed at 500 and 800 °C. The crystallite size synthesized product was found to be around 5–20 nm. FTIR and EDX results were supporting XRD data. Morphological studies represented the spherical nature of Cu0.2Ni0.8O nano-particles annealed at 500 and 800 °C with particle size <70 nm. Electrochemical measurements of Cu0.2Ni0.8O nano-particles annealed at 500 and 800 °C and their nano-hybrids were also performed. Brilliant specific capacitance (303 F g-1) was observed in the case of rGO-based nano-hybrid of Cu0.2Ni0.8O nano-particles annealed at 500 °C. This additional noted specific capacitance was credited to more conducting nature and relatively high surface area of graphene.
| Original language | English |
|---|---|
| Pages (from-to) | 14304-14310 |
| Number of pages | 7 |
| Journal | Ceramics International |
| Volume | 46 |
| Issue number | 9 |
| DOIs | |
| State | Published - 15 Jun 2020 |
| Externally published | Yes |
Keywords
- Doping
- Electrochemical properties
- FTIR
- NiO
- SEM
- UV–Visible
- XRD
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