Effect of thermal ageing on the deformation behaviour of ferrite and austenite in a duplex stainless steel: Micropillar characterisation and dislocation density modelling

The deformation behaviour of the austenitic and ferritic phases in an aged duplex stainless steel is investigated experimentally and numerically. The effect of the ferritic phase's spinoidal decomposition during thermal ageing on the mechanical behaviour of the alloy is studied through micropillar compression tests on the individual single crystal phases before and after ageing, and APT and TEM investigations of the decomposed ferrite and corresponding dislocation structures. Dislocation density-based crystal plasticity models are formulated for the austenitic and ferritic phases, and calibrated from the measured micropillars responses. A considerably higher and more homogeneously distributed initial dislocation density is observed in the austenite, resulting in a more homogeneous deformation of the austenitic micropillars than the ferritic ones. The spinoidal decomposition of the ferrite leads to a considerable increase of its initial flow stress. The strengthening effect of thermal ageing and the resulting localised deformation response of the aged ferritic micropillars are correctly described by the crystal plasticity results, which required a higher initial obstacle (dislocations + inter-phases of the newly formed α^′ domains) density to dislocation motion. Moreover, a strong size effect was observed on the behaviour of the as-received and aged austenitic and as-received ferritic micropillars, but not in the aged ferritic ones. Such contrasting behaviour originates from the fact that, for the size sensitive cases, the dislocation mean free path is controlled by the mean micropillar diameter, whereas in the aged ferrite micropillars, it is by the ∼ 5 nm wide Cr-rich domains within the spinoidal decomposed ferrite.