Abstract
Heat treatment was carried out between 800 and 1200°C to investigate its effects on the microstructure and electrochemical properties of the hollow carbon spheres (HCSs) prepared in high-pressure argon. Samples were characterized by X-ray diffraction, Raman spectroscopy, field-emission scanning electron microscopy, high-resolution transmission electron microscopy and N2 adsorption-desorption isotherms. The graphitization of the HCSs was improved with increase of heat treatment temperature. Mesopores of ca. 4 nm in diameter were created on the HCSs after the heat treatment. The results of electrochemical performance measurements for the HCSs as anode material for lithium ion batteries indicate that the discharge capacity of the HCSs is improved after heat treatment at 800°C compared with the as-prepared HCSs and have a maximum value of 357 mAh/g and still retains 303 mAh/g after 40 cycles. However, the discharge capacity of the HCSs decreases and the cycling performance is improved with the increase of heat treatment temperature.
| Original language | English |
|---|---|
| Pages (from-to) | 1707-1714 |
| Number of pages | 8 |
| Journal | Bulletin of Materials Science |
| Volume | 34 |
| Issue number | 7 |
| DOIs | |
| State | Published - Dec 2011 |
UN SDGs
This output contributes to the following UN Sustainable Development Goals (SDGs)
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SDG 7 Affordable and Clean Energy
Keywords
- Gas pressure
- Heat treatment
- Hollow carbon spheres
- Lithium ion battery
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