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Deformation behavior, microstructure evolution, phase transformation and plastic instability origin of powder metallurgy Al0.8Co0.5Cr1.5CuFeNi alloy during high temperature deformation

  • Minjie Huang
  • , Jufu Jiang*
  • , Ying Wang*
  • , Yingze Liu
  • , Ying Zhang
  • , Jian Dong
  • , Guanfei Xiao
  • *Corresponding author for this work
  • Harbin Institute of Technology
  • School of Mechatronics Engineering, Harbin Institute of Technology
  • Nuclear Power Institute of China

Research output: Contribution to journalArticlepeer-review

Abstract

High temperature deformation behavior of powder metallurgy Al0.8Co0.5Cr1.5CuFeNi (containing BCC, FCC, σ phase) at 1173–1323 K temperature range and 1-0.001 s−1 strain rate range was investigated in detail. Scanning electron microscopy (SEM), electron backscatter diffraction (EBSD) and X-ray diffraction (XRD) were used to analyze microstructure evolution and phase transformation. Transmission electron microscopy (TEM) was applied to examine tiny phase structure. The Arrhenius model and the artificial neural network (ANN) model for predicting flow stress were compared. The ANN model has significantly superior prediction performance. σ phase was dissolved into BCC matrix as deformation temperature increased and strain rate decreased, and Al–Ni rich particles in BCC were greatly dissolved at higher temperature. After deformation, the average grain sizes of BCC and FCC were refined to 5.75–7.32 μm, the orientation of FCC and BCC was quite random, and twins only appeared in FCC. The growth of dynamically recrystallized grains near phase boundary was mutually inhibited. High density dislocation accumulation at the BCC/σ boundary under high strain rate induced the initiation of micro crack. Dislocation assisted grain boundary slip at low strain rate reduced the dislocation accumulation degree at BCC/σ boundary to mitigate stress concentration. This mechanism suppressed the initiation of micro crack.

Original languageEnglish
Article number144373
JournalMaterials Science and Engineering: A
Volume861
DOIs
StatePublished - 19 Dec 2022
Externally publishedYes

Keywords

  • High entropy alloy
  • High temperature deformation
  • Microstructure
  • Phase transformation
  • Plastic instability

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