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三元共晶成分Al2O3/YAG/ZrO2粉体及陶瓷的制备与组织性能

Translated title of the contribution: Preparation, Microstructure and Properties of Ternary Al2O3/YAG/ZrO2 Ceramics Hot Pressed with Eutectic Composition Powders
  • Harbin Institute of Technology

Research output: Contribution to journalArticlepeer-review

Abstract

Al2O3/YAG/ZrO2 powders with eutectic composition have been synthesized by the chemical co-precipitation in alcohol-water aqueous solution and calcination method, and were characterized by X-ray diffraction, scanning electron microscopy and transmission electron microscopy. The precursors were calcined at temperatures of 600~1350 oC in air, and the phase transition process was then revealed with increasing the calcination temperature. Al2O3/YAG/ZrO2 powders calcined at 1300 oC for 1 h consist of α-Al2O3, YAG and c-ZrO2 phases. Al2O3/YAG/ZrO2 ceramics with eutectic composition were hot-pressed at 1550 oC with the above-mentioned powders. The Al2O3/YAG/ZrO2 ceramic sintered at 1550 oC contains an intragranular microstructure, and exhibits a relative density of 98.8%, a room-temperature flexural strength of 420 MPa, a fracture toughness of 3.69 MPa·m1/2 and a high-temperature (1000 oC) flexural strength of 464 MPa. The formation mechanism of an intragranular microstructure in the Al2O3/YAG/ZrO2 ceramic has been proposed.

Translated title of the contributionPreparation, Microstructure and Properties of Ternary Al2O3/YAG/ZrO2 Ceramics Hot Pressed with Eutectic Composition Powders
Original languageChinese (Traditional)
Pages (from-to)288-293
Number of pages6
JournalXiyou Jinshu Cailiao Yu Gongcheng/Rare Metal Materials and Engineering
Volume47
StatePublished - 1 Jul 2018

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